[GSAS-II] Different profiles for different phases
Bartłomiej Gędziorowski
gedzior at agh.edu.pl
Fri Sep 6 07:08:49 CDT 2019
Hello Everybody,
first of all I'd like to say hello to everybody, because this is my
first post in this list. My name Is Bartłomiej Gędziorowski, I work at
AGH UST in Cracow, Poland and I'm a materials scientist.
I worked few years with GSAS+EXPGUI, now from some time I'm migrating to
GSASII and I cannot find one feature. It is the setting of different
profile sets for different phases for a single histogram. I have a
sample in form of a thin layer on a beryllium substrate. As a result on
diffractograms I can see both my material reflections, quite wide
because of sub-micron grains, and very thin beryllium. This causes a
problem, because I cannot find suitable set of profile values for
double-phase refinement. I worked it around putting beryllium
reflections in the background, but that's not a good solution for me.
The beryllium peaks are very helpful, because they allow to precisely
fit sample displacement - we use special in-situ cell in which placing
sample in right position is challenging and we always have some shift.
For that reason it would be perfect to do a double-phase fit.
I would be grateful for some suggestions how to solve my issue.
Best regards,
--
Bartłomiej Gędzioroski, Ph.D.
AGH University of Science and Technology,
Faculty of Energy and Fuels,
Department of Hydrogen Energy,
al. Mickiewicza 30
30-059 Krakow, Poland
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